Ukusebenzisa iphedi yokuchukumisa

Ukuqaliswa kwekhabhoni esebenzayo

Sithatha ingqibelelo kwaye siphumelele njengomgaqo wokusebenza, kwaye siphatha lonke ishishini ngolawulo olungqongqo kunye nenkathalo.

Ikhabhoni esebenzayo (AC) ibhekisa kwimathiriyeli enekhabhoni ephezulu eneporosity ephezulu kunye nesakhono sokurhweba esiveliswe ngamaplanga, amaqokobhe ekhokhonathi, amalahle, kunye neecones, njl. njl. I-AC yenye yezinto ezisetyenziswa rhoqo kwimizi-mveliso eyahlukeneyo ukuze kususwe izinto ezingcolisayo ezininzi. ukusuka emanzini kunye nemizimba yomoya. Ukusukela oko, i-AC idityaniswe kwimveliso yezolimo kunye nenkunkuma, ibonakalise ukuba yeyona ndlela ilungileyo kwimithombo engahlaziyekiyo esetyenziswa ngokwesiko nexabisa kakhulu. Ukulungiselela i-AC, iinkqubo ezimbini ezisisiseko, i-carbonization kunye nokusebenza, zisetyenziswa. Kwinkqubo yokuqala, i-precursors iphantsi kokushisa okuphezulu, phakathi kwe-400 kunye ne-850 ° C, ukukhupha zonke izinto eziguquguqukayo. Ubushushu obuphezulu obuphezulu bususa zonke iinxalenye ze-noncarbon kwi-precursor efana ne-hydrogen, i-oksijini, kunye ne-nitrogen ngendlela yeegesi kunye ne-tar. Le nkqubo ivelisa i-char enomxholo ophezulu wekhabhoni kodwa indawo ephantsi kunye ne-porosity. Nangona kunjalo, inyathelo lesibini libandakanya ukusetyenziswa kwe-char eyenziwe ngaphambili. Ukwandiswa kobungakanani bepore ngexesha lenkqubo yokuvula kungahlelwa ngokwesithathu: ukuvulwa kweepore ebezingafikeleleki ngaphambili, uphuhliso olutsha lwepore ngokuvula okukhethiweyo, kunye nokwandiswa kweepore ezikhoyo.
Ngokwesiqhelo, iindlela ezimbini, ezomzimba kunye neekhemikhali, zisetyenziselwa ukuqalisa ukufumana indawo enqwenelekayo yomphezulu kunye ne-porosity. Ukusebenza ngokomzimba kubandakanya ukusebenza kwe-carbonized char usebenzisa iigesi ze-oxidizing ezifana nomoya, i-carbon dioxide, kunye ne-steam kumaqondo aphezulu (phakathi kwe-650 kunye ne-900 ° C). Ikhabhon dayoksayidi idla ngokukhethwa ngenxa yobume bayo obusulungekileyo, ukuyiphatha lula, kunye nenkqubo yokuvula elawulekayo malunga ne-800°C. Ukufana kwepore ephezulu kunokufumaneka kunye nokusebenza kwe-carbon dioxide xa kuthelekiswa nomphunga. Nangona kunjalo, ekusebenzeni ngokomzimba, umphunga ukhethwa kakhulu xa kuthelekiswa nekharbon diokside kuba i-AC enendawo ephezulu inokuveliswa. Ngenxa yobungakanani bemolekyuli encinci yamanzi, ukusasazwa kwayo ngaphakathi kwesakhiwo se-char kwenzeka ngokufanelekileyo. Ukusebenza ngomphunga kufunyaniswe kujikeleze kabini ukuya kathathu ngaphezulu kwekharbon diokside eneqondo elifanayo loguqulo.
Nangona kunjalo, indlela yeekhemikhali ibandakanya ukuxutywa kwe-precursor kunye ne-activating agents (NaOH, KOH, kunye ne-FeCl3, njl.). Ezi arhente zisebenza njenge-oxidants kunye ne-dehydrating agents. Kule ndlela, i-carbonization kunye nokusebenza kuqhutyelwa ngaxeshanye kwiqondo lokushisa elingaphantsi kwe-300-500 ° C xa kuthelekiswa nendlela ebonakalayo. Ngenxa yoko, kuchaphazela ukubola kwe-pyrolytic kwaye, emva koko, kubangele ukwandiswa kwesakhiwo se-porous esiphuculweyo kunye nesivuno esiphezulu sekhabhoni. Izibonelelo ezingundoqo zemichiza ngaphezulu kwendlela yokwenyama ziyimfuneko yobushushu obuphantsi, ulwakhiwo oluphezulu lwe-microporosity, indawo enkulu yomphezulu, kunye nexesha elincitshisiweyo lokugqiba ukusabela.
Ukuphakama kwendlela yokusebenza kweekhemikhali kunokuchazwa ngesiseko somzekelo ocetywayo nguKim kunye noogxa bakhe [1] ngokubhekiselele apho i-microdomains ezahlukeneyo ze-spherical ezijongene nokusekwa kwee-micropores zifumaneka kwi-AC. Kwelinye icala, i-mesopores iphuhliswa kwimimandla ye-intermicrodomain. Ngovavanyo, benza i-carbon activated from phenol-based resin by chemical (usebenzisa i-KOH) kunye nokusebenza ngokomzimba (ukusebenzisa umphunga) (Umfanekiso 1). Iziphumo zibonise ukuba i-AC edityaniswe ngokuvula i-KOH inommandla ophezulu we-2878 m2/g xa ithelekiswa ne-2213 m2/g ngokuvula umphunga. Ukongeza, ezinye izinto ezinje ngobungakanani bepore, indawo engaphezulu, umthamo wemicropore, kunye nobubanzi bepore avareji zonke zifunyenwe zingcono kwiimeko ezisebenzayo ze-KOH xa kuthelekiswa nomphunga osebenzayo.

Umahluko phakathi kwe-AC elungiselelwe ukusuka kwi-activation ye-steam (C6S9) kunye nokusebenza kwe-KOH (C6K9), ngokulandelanayo, ichazwe ngokwemodeli ye-microstructure.
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Ngokuxhomekeke kubungakanani bamasuntswana kunye nendlela yokuyilungisa, inokwahlulwa ibe ziindidi ezintathu: i-AC enamandla, igranular AC, kunye nebead AC. I-AC ene-Powered yenziwe ngeegranule ezintle ezinobungakanani be-1 mm kunye noluhlu lwe-diameter ye-0.15-0.25 mm. IGranular AC inobungakanani obukhulu ngokuthelekisayo kunye nommandla ongaphantsi wangaphandle. IGranular AC isetyenziselwa isigaba solwelo esahlukeneyo kunye nesigaba segesi yosetyenziso ngokuxhomekeke kumlinganiselo wabo. Iklasi yesithathu: i-bead AC idityaniswe ngokubanzi ukusuka kwi-pitch ye-petroleum kunye nobubanzi obusuka kwi-0.35 ukuya kwi-0.8 mm. Iyaziwa ngamandla ayo omatshini aphezulu kunye nothuli oluphantsi. Isetyenziswa kakhulu kwiibhedi ezimanzi ezifana nokuhluzwa kwamanzi ngenxa yesakhiwo sayo esingqukuva.


Ixesha lokuposa: Jun-18-2022